4-METHOXYBENZYLAMINE | Idarubicin /Meobentine

1. STRUCTURE

2. PRODUCT NAME & DETAILS
Product Name	4-Methoxybenzylamine
CAS No	2393-23-9
HS Code	2930.90.70
Molecular Wt.	137.180
Molecular Formula	C8H11NO

3. SPECIFICATION
Physical Appearance	Clear Colourless To Pale Yellowish Liquid.
Refractive Index (20°c)	1.5460
Boiling Point	236-237°C
Total Amine Value	400 - 409
Method of Analysis	METHOD OF ANALYSIS ------------------ DEFINITION: THE TOTAL AMINE VALUE IS THE MG OF KOH EQUIVALENT TO THE BASICITY IN 1 GM OF SAMPLE. PROCEDURE ---------- WEIGH ABOUT 0.4-0.8 GM SAMPLE IN 250 ML CONICAL FLASK. ADD 50 ML OF ISOPROPYL ALCOHOL & DISSOLVE COMPLETELY. ADD 5-10 DROPS OF BROMOPHENOL BLUE INDICATOR & TITRATE WITH 0.25 N IPA-HCl SOLUTION. END POINT BLUE TO YELLOW COLOUR. CALCULATION:                                  NORMALITY*B.R.* 56.1 TOTAL AMINE VALUE=-------------------------                                WEIGHT OF SAMPLE
Moisture Content (Kf) By Karl Fisher	NMT 0.5%.
Method of Analysis	IMSTRUMENT NAME: VEEGO-MATIC-1 (AUTOMATIC TITRATER) PROCEDURE FOR WEF TAKE APPROX. 15 ML ACETIC ACID + 10 ML METHANOL IN K/F CUP(CUP MUST BE IN A DRY CONDITION). FILL THE K/F BURETTE WITH K/F REAGENT & TITRATE THIS MIXTURE UPTO END POINT BY PRESSING START BUTTON. THEN IMMEDIATELY WEIGH DISTILLED WATER AND ADD JUST ONE DROP INTO THE ABOVE NEUTRALIZED MIXTURE AND THEN START TITRATION TILL END POINT. CALCULATION WATER DROP                                       WT. OF DIST.*100 WATER EQUIVALENT= --------------                                        VOL.OF K/F FEOTER (WEF) EAGENT ROCEDURE FOR % MOISTURE AFTER THE WEF IS CALCULATED, AGIN NEUTRALIZE WITH K/F REAGENR. TO THIS MIXTURE ADD ABOUT 0.5-4 GM SAMPLE & TITRATE UP TO END POINT. CALCULATION ===========                      WEF * ML OF K/F MOISTURE=--------------------------                      WT. OF SAMPLE * 10
Density	1.045-1.055 at 20°C
Assay (By Titration, non Aqueous)	NLT 98%
Method of Analysis	METHOD OF ANALYSIS BY TITRATION (NON AQEOUS) WEIGH ACCURATELY 0.11 ± 0.01 GMS OF SAMPLE IN A BEAKER. ADD 50 ML GLACIAL ACETIC ACID AND TITRATE WITH 0.1 N. PERCHLORIC ACID POTENTIOMETRICALLY. 1 ML OF 0.1 N.PERCHLORIC ACID IS EQUIVALENT TO 13.718 MGS OF 4-METHOXYBENZYL AMINE.
Assay (Glc)	NLT 98%
Method of Analysis	METHOD OF ANALYSIS COLUMN: DB-I, 60 MTRS, 0.25 MM ID. CAPILLARY COLUMN. INJECTION TEMP : 280°C DETECTOR TEMP: 300°C OVEN TEMP : 75°C @ 10°C/MIN-250°C PREHOLD TIME: 3 MIN. POSTHOLD TIME : 30 MIN. DETECTOR: FID CARRIER GAS : NITROGEN INJECTION VOLUME: 0.2 microL

4. APPLICATION
5. HAZARD CLASSIFICATION
6. CAPACITY
7. STORAGE CONDITION

Disclaimer

Typical properties should not be considered as specification. Product covered by valid patents are not offered or supplied for commercial use. The Patent position should be verified by the customer. Products will not be supplied to countries where they could be in conflict with existing patents. Products currently covered by valid US patents are offered for R&D; use in accordance with 35 USC 271 (e) (I) Above information is given in good faith and without warrenty.